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I did both nothing changed the pH of the ketone I did external steam distillation if the way I do my meth now I found out the that you have to ad water to the flasks the fistill over how much water di I add to the flasks with within 100g of p2p

I need help I did the reaction one a nice bath from the start the temp did not go above.5celcius only when one addition of nabr it took the temp to 40cekcius for 40secinds to then it went down to 3degrees further addition it never raised the temperature again as I made sure I didn't add as much...

So your saying you are adding water to the reaction mix and distilling it over I'm stead of using using a external source like U have used how much water do.yku add fir 1kg

I put the P2P in the round bottom flasks 2,neck recovery Bend in neck attached to condenser side neck rubber stopper with a hole in the middle glass tube igies there there until the bowl my source if steam pressure cookers I use the to steam distill meth Fb I put the glass tube that pumps the...

I tried steaming it it just released some powder that sat on top of the P2P so I poured of that the power and started again it just cleaning the P,,2,P in that flask it's not blowing it over as it should do I got some P2,P that came over but i expected a lot more than going to DCM extract...

When you say to steam distilled the P2P are you adding lye to it or just steaming the P2P with no lyeI be using external steam distillation from a pressure cooker PTFE tubbing with a glass tube on the end of the PTFE tube the glass tube goes threw a rubber bung onto side neck in to the flask