Don't get this bullshit motion.ig you had your product you will get shards yes it is possible but you have to use Freon as your solvent when you had it it will form shards buy if you use the yeh normal solvents eg toluene you will get powder which has to recrystallised
Easy steam generator pressure cooker on a gas hotplate. So you can adjust the pressure of the steam being pumped into the flask also use flasks with side necks and run the steam through the side necks
And scalling up is easy if doing bulk just need to use 10l and 20l rbf
I just read this properly pH 0 big no no you have to freebase it again and your going to loose product also from looking at your beaker you have belted it when doing distillation and brought caustic over with your oil when doing Distillation wether simple or steam no further than a quarter of...
Don't listen to those *****heads sayi
3ng this post isn't true
1 sodium thiosulfate is used to kill any iodine and color when doing rp/hi route that's why I tell people to use hypophosphorous acid as you don't have to filter the red phosphorus out and use sodium thiosulfate and you don't have...
Before they *****ed the Sudafed pills with gaks etc a 1000 boxes of Sudafed in a 25 litre plastic white food grade bucket first wash 12 l of methylated spirits hot in the the bucket paint stirrer on a cordless drill stir untill all is disolvedl place the bucket on a bench with the lid on it...
I know your not suppose to do this bit I have added more methylamine hcl and lye then used mgso4 then I quickly vacuum filter the the solution and then quickly poured it back into a fresh clean 10l rbf that i did the synth then added the p2p and nabh4 and it worked no dramas
All you had to do was separate the fb oil from the caustic water in. A sep funnel wash the fb oil with equal amount of dh20 discard the dh20 then add equal amount of anhydrous acetone tritate with hcl acid til pH was 5.8 add 1ml of dh20 to every gram of meth hcl then evap before you get a...
To do these you place the tabs in a sifter pore warn water over them inti all the white part has dissolved off them place the brown part of the tabs on paper towing to dry once try crush all the brown tabs up and place in a beakef and give them 3 hot toluene washes to get rid of the wax and...
Once you had your freebase you should of disolvedl in 2 to 1 mix of acetone /,free base then tritated with hcl acid to pH 5.5 to 5.8 the evaporated to give you your product also half if that is garbage lmeth so you have to do a resolution with tartaric acid to get the dmeth