This is intermediate part of this process. Later all watery layer on the bottom turns to a kind of "porridge". Wasting of time. Also such long exposure at high T evaporates some stuff. I lost around 20 gr of 250 gr pure powder.
I have some other ideas. Will try as I get inspiration.
You can check PH of this "oil" at any time. But i think it is water: two layers formed, one on the top, another one on the bottom. Water somewhere at the middle.
Water inside i guess. Solubility grows noticably at 40-50C.
It looks you got the result, similar with crystals I got here. Some crystals are normal (but small), some crystals (from inner layer) are "watery crystals"...
I tried to repeat this procedure with slow temp reducing. And I'm 100% sure - hotplate doesn't work.
Look, there is a hot surface of the plate on the bottom, and cold air on the top. It means, nucleation doesn't start at the bottom - bottom is more hot, so no chance.
As the result, thin crystal...
Now I have 100% evidence long time exposure of MDMA at high temperature affects the color.
I use different crystallization methods and it is not a problem for me to get pure white crystals. Normally it doesn't take a lot of time for heating, and crystals are perfect white.
But this time I...
Bro, relax. Do you think I'm a schoolboy junky cooking meth for living source? I was graduated in math, not in meth. So, why you believe you can impress me with your graph?
Bro, it looks you worry about 120 EUR for your fake tests too much. Relax, bro. It is the only of your incoming? I can hire you as a drop maker if so: send me PM, I will find a job for you.
Come on, guys! I'm not angry, I'm laughing. I spent a few hours of my life breaking my brain and thinking about this riddle. I supposed many different reasons including MDM-imines building colloids with excess of isomers of amines. Holy *****, this is *****ing 5-10% margin error!!!
I'm laughing...
Oh, no, bro, not to energy control, please. You remember i shared with you test result 87%? I did a few tests more.
87% not again, but always))))))
Most fun explanation: error margin 5-10%.
In other words, guys, it is simple blah blah blah human error blah blah blah, and I paid 360 EUR in total for nothing. Many thanks for great service.
Of course, it is questionable result, and main question is: "Why do I need to pay 120 EUR for a sample testing with margin error 5-10% if I can...
Had a few attempts to collaborate with Energy Control in harm reduction realm and safety. More than questionable.
First of all you have wait to get your result at least 3-4 weeks from shipping date, and 2-3 weeks from delivery date. First sample took 3 weeks from delivery date, that is out of...
When I was *****er, my friends involved in clandestine chemistry did as below:
1. battery electrolyte taken and put on the stove for evap. Evaporation continues till density 1.8 gr per 1.0 ml reached.
2. Some glass vessel with hose prepared, and NaCl (kitchen salt) placed inside.
3. Obtained...
Ah, sorry, got your problem. A bit of theory if so, bro.
Acetone has a unique property: it solves a lot of mdma hcl at 50C (1 gr of mdma hcl per 2.5 gr of acetone i guess) and almost zero if acetone is frozen. This property is related with "vacuum permittivity". Vacuum permittivity of acetone...