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I used the Vevor kit to distill sulphuric acid in my balcony. It proved durable. Used 2L flask with heating mantle (It must be able to go to 400 C). Distill 1.8L battery acid or pool pH down that contains H2SO4. At first the water comes out (containing ~1% H2SO4). You have to keep increasing the...

Couldn't log in for long time. The reaction went! After 6h at 60 C bath I rised the temperature to 100 C. The solution turned clear reddish and I kept it in bath for another 5h. About 6h after taking it out I noticed it had turned cloudy. Another 5 hours and the layers had separated. I wondered...

My reaction won't go. I used 20ml Cyclohexylamine (99.5+%, <0.3% H2O), 100ml Benzaldehyde (99.8%, Pure, FCC, Food grade), 40ml GAA (99.8-100.5+%) and 100ml Nitroethane that I distilled from Acrifix 1S 0117 solvent based adhesive. I don't think I got rid of the Butan-1-ol (1-<3%, BP 117.7 C) it's...