Search results

Rocks yes we want to make rocks Its racemic keta ye, not S

No evaporation doesnt yield the solid rocks. It yields a crystalcake of small needle-like crystals indeed. Tried freeze method and yielded bigger shard-like crystals like i posted before, but still.no rocks...

No it doesnt need evaporation before freezing, does it?

I tried untill satured in boiling water/methanol and then how they said it in the thermos way but no rocks

@bigusdickus I tried with the freezer/thermos technique. But im still failing to produce rocks... Im not going past the shardlike shapes like this

I also hear the yellow waxy one has less yield, but we will see after test

Yes washing after is prefferable as the oil is going to contain less contaminants. But ye i also know people who just yank the oil straight into the reactionvessel after conversion.

1kg P 1kg water 150gr NaOH Mix and melt at 85/90 for 1hr 450gr Phos and again 1,5hr at 85/90 After should be immediate separation from the layers

White powder starting material was this test, i also have sample from yellow waxy lumpy powder. Swim will do a small testconversion tomorrow also on phosphoric acid...

Swim already succeeded the testconversion on phosphoric acid with 500gr of 28578

So swim can use 316-steel for the conversion and not glass or plastic.

Hey everyone, Anyone has tried this conversion with phosphoric acid instead of HCl? I got this pathway 1kg 285 1kg water 150gr NaOH After 430gr phos

Thats what i think too, its only 1,5hrs and the hcl is very diluted with water and there is also caustic to neutralize a part. Its not like with 5449 that needs 5 hrs with stronger solutions But if someone has xp with this let me know, swim starts saturday conversion

Totally different question about this conversion... Hope u have an answer Swim is going to do this conversion but his ptfe stirring rods for mixing havent arrived yet. Can he for once stir with a 316 steel stirrer for once maybe for 1.5 hr? I know the hcl eats away the 316 but doesnt matter...

Yes i have stumbled on a piece of text describing this... Going to need to be creative doing this large scale. Many thanks for the pointer...

Swim too is familiar with this problem, doest seem.to crystallize. Even after trying to recryss, it keeps coming out thick and oily. It is active as fk though...

Nembutal is a barbiturate

https://www.khanacademy.org/math/get-ready-for-algebra-i

B-oil is streetslang for BMK

Great work bro, a little research comes a long way...