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Can it also be used for the one Pot Synthese (NabH4 + CuCl2) ?

Ok thank you very much

I know that, but I've heard that the distillation is faster if you do it in a vacuum, in this case with water, is this right?

Is it possible to destill amphetamin freebase in vacuum without adding of water like in a normal steam destillation? If yes, can it be done in a rotovap and on whitch temperature is the boiling point, for example at 100mbar vacuum ? Does anybody know?

Hey guys! At what speed are you stirring during the synthesis and is it a constant stirring?

After dozens of successful syntheses, it actually failed for me this time. my glass reactor had a small crack which unfortunately led to a large one and has therefore become leaky. Luckily this happened shortly before the addition of CuCl2. I then stopped the synthesis, quenched the reaction...

What do you use for external heating to keep the temperature on 80 °c for 30 mins?

possible to do the vacuum distillation with a pump with the following specs: Flow rate (max.): 5.5 l/min. Ultimate vacuum (max.): 160 mbar (abs.) and what would be the boiling point of the IPA with ussage of this pump

What is the best way to carry out an extraction with such big quantities, stir well and then decant? and does the distillation have to be carried out in a vacuum or can the IPA also be distilled off in the normal way? Sorry for the last writing in german, didnt see that autotranslator was on

Das würde mich auch sehr interessieten

Can the recipe be scaled, for example with 50g P2NP: 60g aluminum foil, 500ml IPA 250 GAA. Or do you have to calculate it specifically for the amount of 50g P2NP? Can 70-80% AA also be used?

First off all thank you very much for these very interessting synthesis route. Is a 30l glass reactor useable for this way? (Something like that u see on the picture) And how do you realize the stirring? Are you using a electrical overhead stirrer?