Search results

  1. D

    Can cocaine even more purified by re oxidation ?

    Since i own a centrifuge(or build one out of old drone motor) i'll give it a try. To come back to the actuall topic and Answer my own question. Yes, cocain can be reoxidized for purification. See https://www.emcdda.europa.eu/publications/eu-drug-markets/cocaine/production_en#figure1 Just...
  2. D

    Can cocaine even more purified by re oxidation ?

    Can you explain how does soubility work ? I can find sources stating 2.7 - 3.2 ml ethanol can dissolve one gram. If i try with up to 4 ml per g. The stuff remaining in filter still tests positiv with morris reagent. My theory is there is some kind of sugar mixed in. The sugar can dissolve in...
  3. D

    Can cocaine even more purified by re oxidation ?

    Wow, thanks for the friendly and respectful response. I'm sure we can find better ways to purify. Was the water recrystalisation that you meaned with "I can give you a scheme that will actually leave practically no trace of adulterant, " ? If I look in my notebook i tried it already 6 times...
  4. D

    Can cocaine even more purified by re oxidation ?

    These and some more are all cleanings teks you can find on the internet. But you right i've no idea what happen on molecular level. I'm not a chemist. But i realy like learing alll these things and get rewarded with good blow. Actually i spend more money on eqipment and chemicals than i want to...
  5. D

    Can cocaine even more purified by re oxidation ?

    Okay, i'm unsure about the Ehrlich reagent. It is not supposed to become green... The other give mixed signals.
  6. D

    Can cocaine even more purified by re oxidation ?

    Hi, currently i'm struggling with finding a decent source. Even after 1.Aceton Wash 2.Ethanol Recrystallisation (i speed up the filtration with vaccum could that be a problem?) 3.Convert to Base 4. Hexan L-L Wash 5. Convert to HCL Again 6. Second Ethanol wash I end up with at least 4 very...
  7. D

    Seperate Cocaine and Meth

    So, there nothing i can do? Of course i will find a different source because of this, but nobody likes chemical challenges? What would happen if i added very small drops of solvent to a great mass of powder mix and pipette on a surface? The stuff solved by solvent should change from drop to...
  8. D

    Seperate Cocaine and Meth

    More than 1 gram
  9. D

    Seperate Cocaine and Meth

    Hi, i got batch of cocaine which is unfortunately cut with Meth. The Simons color test confirmed that. Since both are very souble to water the cold water method doesn't work here. I tried to find a solvent but both seems to be identical. This is what i found for information. Cocaine...
  10. D

    cocaine crystallization/purification

    We had the some topic here. I solved it by putting it in acetone to make solid again.
  11. D

    Maximum temperature for cocaine recrystallization with ethanol

    Sad Story :( I'm thinking about designing some parts that can be 3D-Printed for making A/B easier. It's look like you already did the some of the experiments i'm currently doing. What cocain purify teks can you recommend ?
  12. D

    Maximum temperature for cocaine recrystallization with ethanol

    I bought a frit buchner not so long ago. Purifing stuff realy takes people into buy glassware :D If i get you right i don't need other techniques like acetone wash, A/B extractions etc. ? I only need to master the cold waterthing?
  13. D

    Maximum temperature for cocaine recrystallization with ethanol

    The same happened to me. If you get brown goo after some point, you need to smear this in acetone. I use my kitchen sc*****r and an dental pick for that. The acetone will make the goo hard and crystal looking again almost instant. Crush the solid block while in inside acetone to get everything...
  14. D

    Maximum temperature for cocaine recrystallization with ethanol

    I will try the could water way next time. Thanks :) I'noticed something. I don't aktually need to wait for full crystallisation. You can start scraping as soon the ethanol is evaporated. I use 55 °C for this. At first it will be all like goo but it will start to build crystals and powder in no...
  15. D

    Maximum temperature for cocaine recrystallization with ethanol

    Okay, i did now a lot of expirements and can say if you heat your cocain over 70 °C you will break it. But if you stay below 60 °C you can speed drying speeds alot up. Eg. i can do an aceton wash with in minutes. The result will be confortamble to consume. The important part, is that you need to...
  16. D

    Maximum temperature for cocaine recrystallization with ethanol

    Hi chem experts, after washing cocain with 96.5% (190) ethanol i speed up the drying process via heated plate(3D printer bed) and a normal houshold fan. Normally the tutorials recomend 24-48h drying process but with 50-60 °C heat it is a matter of few hours. Do i degenerate my cocaine with that...
Top