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I wonder what it is about 3-cmc that it seems it's preferable to work in the aqueous layer instead of the organic layer when doing acidification. I also tried your method @Jesse_Pinkman_ and had good results working the aqueous layer. When working the organic layer, I never get salt, just...

Be careful when using a digital ph device and DCM, if you leave it in the rm while monitoring it will melt the device.

For hexadrone, I would assume the standard methylamination with a solvent (dcm .ea, nmp) ? I don't have any pyrrolidine around.

Hi Everyone, I was shipped 2-bromo-1-phenylhexan-1-one by mistake. What can be synthesized with this? I can't find much information on this precursor.

Well according to other sources, DMSO would be a good solvent to use. I will try it and report back.

I enjoy it only In very small microdosing quantities. ~30mg. It's closely related to a popular antidepressant Wellbutrin. I don't think it's a good substance to get seriously geeked on.

What are the two solvents? Are they any of chloroform, ethyl acetate or methanol?

Does 2b3c react with DCM? Is that why DCM should not be used? Is Toluene a better solvent? If not Toluene, what other solvent should be used?

Hi Everyone! I'd like to synth 3-cmc for personal use. I've become quite fond of it, but can no longer obtain it (constant fraud / poor substitutes). I have a little bit of organic chemistry experience, such as simple acid base extractions, etc. I've perused this forum and there are several...