THIS
"The solution was cooled and extracted with xylene. The solution was filtered and the filtrate washed with xylene and the xylene portions added together. About 100 mls of conc HCL was added to the xylene shaken and separated. The aqueous solution was extracted with xylene and the xylene...
, High Yield MDAEasy, High Yield MDAExerpt from something I heard somewhere.......The Finkelstein reaction is the word for the day! Bromosafrole in acetone treated with KI to form the iodide (iodine is a much better leaving group). Iodosafrole forms the amine with NH3 alone at normal pressure...