I’ve tried this reaction with these exact ratio’s, and I just can not seem to get any p2p. I am following the procedure exactly - as hard as it is to get my addition funnel to drip that slow, I’m matching every parameter.My solution turns green. The RBF is a mess that I can hardly see in. I...
Hate to be the one to break it to you, but big pharma looks like they’ve solved the SnB issue once and for all. They’ve introduced a supergak that will gum up the reaction even if you’ve cleaned up the pills into needle-like crystals.
What does this mean?
To put it bluntly - , you’ll never be...
I'm having the exact same result on all of my attempts at a one-pot methamphetamine synthesis following the procedure found HERE.
Everything seems to go well, but when I gas my non-polar, it clouds the solution the instant my tube goes into the flask. The precipitate isn't crystalline at all...