Search results

i want to ask if any of you have experience with best method and rates and tempratures for the reduction , i specifically talking about 2,5 dimethoxy-NS to 2ch lets say something like this my friend tried. A 2 neck round bottom flask containing a 1:1 mixture of IPA:water by weight (250g/10g...

i cant get 48% hbr from a seller , so i want to ask if its possible , will it work ? because i did brominate 2ch like that , so i wonder , and if so and what ratio and what scale will it work.

just put a balloon on the condenser , it will keep the pressure the same in the RV

dude i dont know why the insisnt on nmp in this forum , dcm with give you much higher yields and easier workup , dcm can yield 70-80% where nmp can be anywhere with 20-50 %

for 5 meo tryptamine sutff , 5 meo dmt , 5 meo mipt , 5 meo dipt and such , i try to make 5 meo mipt trough reductive amination

can answer but where one would get mercury?

if you get blue product it means there is too much methylamine in your organic layer , wash it with salt water 5 times and acidification should go better

the blue color is methylamine residue i think , i did the reaction and all went well until acidification also , then powder participated and after x<ph 7 it turned blue , but i was able to wash the powder with acetone and it became white maybe you didnt add enough water to dissolve the...

did you find out why it was blue? , i followed the sythesis with 25g of bk4 and after adding 1:1 hcl acetone to the RM at one point it kinda solidefiend for a sec , then redissolved , then turned blue and bluish poweder praticipated ,

750g is a good yield i hope i can get this much. when you refer to dcm\toluene , you mean the sythesis from 4mp right? because if you use bk4 then its only and extractor and temp doesnt matter

So lets try to figure stuff out so we wont waste precursors. we have 2 ways 1. from 4MP we brominate -> methylation or we skip bromination and get 2br4mp and just do one reaction. i saw various posters run into trouble so we will try to solve the problems one by one. Synthesis...

sorry forgot to quote . my product came out not silver gray buy sparkly yellowish sand in hcl form , does it look correct?

how does the product looks ? is there a picture? my product kinda looks like sand , even after washing few times , crystaline sand

can the nmp be recycled?

8. Discard the water top layer. 9. Put again in the reactor the oil top layer. how many layers will there be? the top was discarded water and then ?

its also very potent a dose is 5-15 mg

yeah so i posted a way with the hand written chart , looks viable ? they make it somehow in the netherlands and the drug is not expensive so i guess they have a good way

Thanks for saving us time ! just got mine , so just in time. thanks a lot !

wouldnt that be 6-Bromo-1-benzofuran for 6 apb ? this one i searched and can get few grams for 1000$ :(