Rollin88,
I think your problem is the pse itself combined with needing dry HCL gas. The 24hr tabs have povidone in it that will rob your goodies! It must be steam distilled prior to reaction. Also if you are not bubbling HCL from RV through another stop through more SA it will be wet when gas...
Hello Patton, bear with me please as this is my first comment, or question rather. I have tried repeatedly to purify mamph by recrystalization, and failed miserably. I just keep wasting product. I am struggling please help with a process! This was my last attempt in attached file.