Well...after some fails, i think i have done finally... thee result are clean oil, no dirty stuff..no more honey look, but with a big difference if we compare with methyl pmk, the result colour is an brown-dark red oil, with an intense sassafras smell which keeps the state in room temp, and...
Thanks for your answer. Maybe I was unclear but what I meant was that I did it in 2 steps. First naoh (and let it sit for at least one hour) and after that the reaction with HCL. Where after adding the the HCL it separated in to two layers.
With the old powders I never distilled them and was...
I’m having the same issue with the wax. After saponification and reaction with HCI a nice light brown coloured oil comes out. After letting this cool off to room temperature it turns dark brown, almost black and thick.
Anyone has input on this?
Including crystallization the process will take 5 to 7 days.
You can work with methylamine in water, in alcohol or methylamine hcl.
I just saw there is a seller here on the forums for Methylamine. You might check that out. I don't know how legit he is though.
I'd say Mono-Methylamine and NaBH4 is the easiest to go with. Not much knowledge and (special) equipment needed.
Only issue with this route is that final product contain significantly more impurities then with other methods.
Nevertheless, in my point of view still a very potent result. If...
There is a difference between PMK and BMK glycidate. To get mdp2p you need P glycidate. Are you (sure you're) using PMK?
Also there are different types of P on the market right now, so it would be important to know which one you have.