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MDP2P 100G. 72% from Heliional, easiest. How to synthesize MDP2P from Heliional using a readily available and non-hazardous precursor?

What I want to know is whether this method works or not. And how much acetic acid should be used per 20 grams of nickel oxide (black)? And what is the temperature of the reaction mixture? And should I wear protective equipment? How many hours does it take in total?

I found this method and he wrote: Nickel Acetate 20 grms of nickel oxide (black) is dissolved in Acetic acid and heated with stirring until the mixture turns pale green. The excess Acetic is drained off , the rest is dried and powdered.

I just want to ask someone who knows the methods and details. To synthesize nickel acetate using old and obsolete methods.

I don't have that many expenses. And I like to synthesize substances and make my own.

Hello friends Who knows how to prepare Nickel(II) Acetate 100g.?

What's the right way to prepare 40% aqueous methylamine solution?

I'm sorry, but I really don't know what to do. And in my country there is not much knowledge about chemistry. I'm sorry for how stupid my question was. But I need help and want to know what I need to do and what to do next. Thank you for the answer.

I've checked out the tips and how-to from The-Hive. And I found different ways. Plenty to crystallize it. But I don't know what to do next.

I failed at the last step. And I don't know how to crystallize MDA from the aqueous phase.

Yes it works. I'm having trouble with separating the salt from the mda in the end? I don't understand the same thing as work up as usual? Can someone explain? I tested what I do have, black and smokes instantly.

"The solution was cooled and extracted with xylene. The solution was filtered and the filtrate washed with xylene and the xylene portions added together. About 100 mls of conc HCL was added to the xylene shaken and separated. The aqueous solution was extracted with xylene and the xylene...

Preparation of 35-40% methylamine aqueous solution. Could you please tell me what the mixing ratio is? thank you

Hello friend, I have a question. In the last step you just use (NaOH) in case it crystallizes, right? And the .PH value should be 7.5, right? I don't know much about chemistry. If I'm going to confess, it's that I don't know. After adding the substance (NaOH), what must be done to get MDA? I...

Hello friend, what do you use? What method is used to synthesize MDA? Could you please tell me? about the synthesis process and details of your chemicals

I am preparing to set up a small laboratory. But I haven't done it yet. Does this method work? or it failed

Hello friends. I have a question 1. In the final step, you use the crystallization method with a stream of HCl gas. Is that right or does it burn? 2. Amide. 100 g aldoxime is mixed with 300 mL xylene and 2 g nickel acetate, added and refluxed for 5 hours. Distill approximately 100 mL xylene...

thank you

You mean this one?= The amines are then released from the aqueous phase with a NaOH solution (45 g of NaOH in 135 mL of water). The oil is separated with ether (or toluene, methylene chloride, etc.). It is then converted to HCl salts along the HCl gas stream. The crystals formed from the ether...

The solution was cooled and extracted with xylene. The solution was filtered and the filter was washed with xylene and the xylene fraction added together. Then, approximately 100 mL of concentrated HCL was added to the shaken xylene and separated. An aqueous solution is also extracted. Xylene...