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  1. TheVacuumGuy

    Im looking for sulfuric acid 96-98

    Looking for a vendor 
    I can walk into almost any store and get methylamine 😋 But a hole in your knee in 10 seconds is maybe what you *thought* have happened. Unless it spoiled in your face or somewhere between the legs, you can finish what youre doing and do the rinsing a minute later. If it were nitric acid, make...
  2. TheVacuumGuy

    nice and efficent route for self 2b4m syntehsis (avg 50 usd a kg)

    H3po4 with NaBr to produce HBr? Going to try this in a minute. Got plenty HBr, but just curious if the 2 react.
  3. TheVacuumGuy

    Failed 4mmc synthesis, need help

    Question 
    Thin red top 🤩
  4. TheVacuumGuy

    4mmc synthes in ethyl acetate

    Sidenote: I have no degree in chemistry. What I described above is just my experience and may, or may not be, scientifically correct.
  5. TheVacuumGuy

    4mmc synthes in ethyl acetate

    I dont care about yield percentage game since it's all margins talk. I'll explain below. To your question: when done correctly, ~55% is possible. Acidification process is more or less the same. Check out the Video (and thread), and New thread More than yields, I care about failures. And in...
  6. TheVacuumGuy

    Failed 4mmc synthesis, need help

    Question 
    Are you sure about that, or is the recipe wrong?
  7. TheVacuumGuy

    Failed 4mmc synthesis, need help

    Question 
    That green happens when it's either too hot (not noticing solvent boiling due to stir), or sitting too long (eg: in ethylacetate for 6 hours), but mostly a combination of those. I've had this twice and both occasions I fell asleep.
  8. TheVacuumGuy

    4mmc synthes in ethyl acetate

    Yes. Without triethylamine. But despite its speed, this is not a route I use regularly.
  9. TheVacuumGuy

    Pre-ban Cathinones. Unable to replicate. [bounty!]

    3-mmc is cleaning up your house with a smile and horny as *****
  10. TheVacuumGuy

    Pre-ban Cathinones. Unable to replicate. [bounty!]

    Yes, what i sent first time was 3-mmc, and this time sent 4-mmc. They differentiate very well.
  11. TheVacuumGuy

    Pre-ban Cathinones. Unable to replicate. [bounty!]

    I submitted a sample of some recent self-made mephedrone to the lab and it came out 93%, which suggests higher purity than the commercial preban sample . So now I'm even more confused since this tastes so soft, no throat hit, effects are less. I would, without hesitation, trade in 1 kg for...
  12. TheVacuumGuy

    🔍 Most Wanted!

    Just use correct (own) details. You attract more attention by using empty addresses, mailboxes or other constructions. If they want you they'll get you anyway. Make sure you know local law, and make sure you have a "somewhat" plausible story
  13. TheVacuumGuy

    🔍 Most Wanted!

    Discounter is my home supplier 👍
  14. TheVacuumGuy

    🔍 Most Wanted!

    Wh wingroup was banned here after multiple issues with them. So please don't recommend them.
  15. TheVacuumGuy

    Mephedrone synthesis (4-MMC) in NMP solvent. Large scale.

    If you buy electric, do yourself a favor by spending extra to get a glas probe. Otherwise it will dissolve (yes, been there)
  16. TheVacuumGuy

    4′-Methylpropiophenone bromination to 2-bromo-4'-methylpropiophenone. Large scale.

    how to get it crystallized? When creating a saturated solution in isopropanol, and letting it stand, the entire content will "crystallize" (with multiple wet inner parts)?
  17. TheVacuumGuy

    Alternatives and substitutes

    If you live in the usa as you say, you should be able to get sulfuric acid easily. You can get sodium-nitrate easily. So you can get fuming nitric acid easily by adding the acid to the salt and setup for simple distillation (apparatus should tightly assembled using grease to minimize fumes...
  18. TheVacuumGuy

    4′-Methylpropiophenone bromination to 2-bromo-4'-methylpropiophenone. Large scale.

    Well, I did not follow the procedure 100% which could clarify. I just set it up, adding dropwise and go to sleep. Next morning it was way to hot and I reduced addition. Then 8 hours later noticed that addition has stopped while the mixture was full of crystals and I opened the valve, which added...
  19. TheVacuumGuy

    how long the bromination of propiophenone takes? ( methcathinone project )

    Question 
    Woops. You're asking propiophenone. Sorry. Should work about the same though
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