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You gotta do a little footwork…. You can’t just expect this all to be put in some video in some comprehensive manner. There are textbooks of info that is needed to these procedures safely and that is something that can’t be translated into a video in any complete manner. All the info you seek...

Great video, would love to see the GABA sandmeyer pathway, seems a bit less toxic. But this is great info.

The servers here seem to be hitting capacity most of the time or have a huge latency issue, it’s hard to Get most of the bigger videos to complete a download. There are mirrors of a lot of these videos on YouTube. Some of them are available for download straight from YouTube with a download...

Prices are looking more attractive for these oil less pumps, I was wondering if anyone had any experience with these or if the specs look okay for vacuum distillations? #broke the link to avoid web trackers, replace (.)com with .com...

The acetone should evaporate over time. Spread it out over a drying dish evenly (breaking up any clumps) and it should dry in about 1-2 days or so. you could put it in a vacuum chamber to speed up the process or heat it up on a flask and pull a vacuum for some quicker techniques

Found a 32 fl ounce bottle on eBay a couple months back. :)

I'm curious if they used "Step 6" and not another step in this family of products. AFAIK Step 6 is the only one that is primarily nitroethane. Step 8 has Acetone and Nitroethane. "Cuccio Pro Powder Polish Dip System Step 8 Dipping Powder Remover" Chemical Name % by Weight CAS...

I actually found a bottle of this for my P2NP synth. All I need is N-butylamine now (having some trouble on that front)

I am wanting to do this soon I plan to reduce 4F-P2NP with NaBH4/CuCl2.

Right click the download link and “save link as” usually allows it to finish

AFAIK it is a liquid transfer pump of some sort designed specifically to move liquid and is separate from a vacuum filtration pump (I think) Depending on the scale you’re synthesizing at, chemists wont usually need it and can do without. You can replace all the liquid pumping with more...

No it is a common fuel additive and used in RC cars, though local restrictions may apply for you I’m not sure about your laws

Found it on eBay. Currently in the process of teaching myself how to make it.

You want as close to pure reagents as possible. No you do not want to dilute the sulfuric acid with water, in fact you would want to make sure there is little to no water in the sulfuric acid at all. Your acetone also should be anhydrous (dry) and of decent purity with no other chemicals mixed in

I had p2np flare up after an unintentional quick addition with the nabh4 it didn’t do anything negative to my final product. I filter all the copper compounds out with 2-3 coffee filters after letting it sit after the 80c heating.

I’ve been doing 5g batches every couple of months since last year and I’m just now starting to get some good results. some tips I have is at a small scale like that. Wait into you’ve added the p2np all the way and then heat it up manually to 60c for 30-45 min and the same with the CuCl2 after...

Whatever you do, do it on a mg or gram scale first just so you can see what’s going on. That’s a lot of product to waste if you mess up somewhere.

Would substituting benzaldehyde with 4-fluorobenzaldehyde result in 4F-P2NP?

I tried to but when I went to add acetone to the freebase/DCM extract that I pulled, it would also not crash out when I attempted to salt it. It also created an emulsion layer and separated the DCM and acetone. I suspect I should have evaporated the DCM before adding acetone to the freebase...

This thread on Reddit has a ton of great info on the 5g scale. It was actually made in reference to this thread here in BB. I basically followed it word for word and have been successful. https://www.reddit(.)com/r/TheeHive/comments/12hcbrr/complete_nabh4_copper_salt_reduction_n00b/